HRID465780

反应详情

EQUATION

反应方程式

HRID 465780 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Ethyl pentanimidate hydrochloride (42.66 g, 257.8 mmol, 1 eq), diaminomaleonitrile (27.90 g, 258.1 mmol, 1 eq) and pyridine (400 mL) were mixed and refluxed for 48 hours under N2. The solvent was removed by rotary evaporation.

WORKUP

后处理

  1. temperaturerefluxed for 48 hours under N2
  2. customThe solvent was removed by rotary evaporation