HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthalenecarboxaldehyde → HCID 20386239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthalenecarboxaldehyde | HCID 6201 | — |
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20386239 | HCID 20386239 | 93.4% |
Reaction Steps
Interaction of 15.6 g of 2-naphthaldehyde and 10.2 g of 3-dimethylaminopropylamine in 80 ml. of benzene following the procedure described in Example 1 yields 22.4 g of oily product; boiling point 146°-149° C. at 0.1-0.2 mm. of Hg. The material solidifies when stored in the cold, melting point 29°-31° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04174317 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-5c62bae5abc847c69f9c7ff5d2c4b45f |
| Source note | uspto-grants-1979_11 |