HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2,6-Dichlorophenyl)anthranilic acid → HCID 19815175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2,6-Dichlorophenyl)anthranilic acid | HCID 151812 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Product | HCID 19815175 | HCID 19815175 | 67.2% |
Reaction Steps
According to the procedure of Example 1, 2-[(2,6-dichlorophenyl)amino]benzoic acid (J. S. Kaltenbronn, et al., Arzneimittel-Forschung/ Drug Research, 33(1), 4a, 621-627 (1983)) (4.1 g) is reacted with hydroxylamine hydrochloride (4.04 g) to provide 2-[(2,6-dichlorophenyl)amino]-N-hydroxybenzamide (2.9 g, 67%); mp 171-173° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155110 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-64051e9b3e2c4c1385b85f4a6fa57e98 |
| Source note | uspto-grants-1992_10 |