HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → 4-Benzoyloxy-2-pyridone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 4-Hydroxy-2(1H)-pyridinone | HCID 54696004 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 4-Benzoyloxy-2-pyridone | HCID 14049662 | 44% |
Reaction Steps
50 ml of a solution of 1.00 g of 4-hydroxy-2-pyridone and 1.35 ml of benzoyl chloride in pyridine was refluxed for 6 hours. After the pyridine was distilled off, the residue was mixed with water. The precipitate was recovered by filtration and was washed with a small amount of ethanol to obtain 0.86 g of the title compound in a yield of 44%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155113 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-ff2759b4c10a440087bdb0d6c4f019b1 |
| Source note | uspto-grants-1992_10 |