2-Chlorobenzoyl chloride → HCID 14049666, compound

HRID 466119Notes

Reaction equation

HRID 466119 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][NH:5][C:4](=[O:8])[CH:3]=1.[Cl:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12](Cl)=[O:13]>>[Cl:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12]([O:1][C:2]1[CH:7]=[CH:6][NH:5][C:4](=[O:8])[CH:3]=1)=[O:13]

Participants

3

Reactant 2

HCID 691102-Chlorobenzoyl chlorideHCID 546960044-Hydroxy-2(1H)-pyridinone

Product 1

HCID 14049666HCID 14049666, compoundYield 68%

Procedure

The general procedure of Example 12 was followed using 1.00 g of 4-hydroxy-2-pyridone and 1.36 ml of 2-chlorobenzoyl chloride to produce 1.42 g of the title compound in a yield of 68%.

Sources & evidence

ORD record
ord-e8d69e82bc48414984bb255bbbfe6b7e
Source dataset
uspto-grants-1992_10
Patent number
US05155113

Reaction notes

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