2-Methylbenzoyl chloride → HCID 178424297, compound

HRID 466131Notes

Reaction equation

HRID 466131 reaction equation
C[Si](C)(C)[O:3][C:4]1[CH:9]=[C:8]([O:10][Si](C)(C)C)[CH:7]=[CH:6][N:5]=1.[CH3:17][C:18]1[CH:26]=[CH:25][CH:24]=[CH:23][C:19]=1[C:20](Cl)=[O:21]>>[OH:10][C:8]1[CH:7]=[CH:6][N:5]=[C:4]([O:3][C:20](=[O:21])[C:19]2[CH:23]=[CH:24][CH:25]=[CH:26][C:18]=2[CH3:17])[CH:9]=1

Participants

3

Reactant 2

HCID 702762-Methylbenzoyl chlorideHCID 21819823HCID 21819823, compound

Product 1

HCID 178424297HCID 178424297, compoundYield 44.3%

Procedure

The general procedure of Example 27 was followed using 4.0 g of 2,4-bis(trimethylsilyloxy)-pyridine and 2.92 g of 2-methylbenzoyl chloride, thereby producing 1.59 g of the title compound in a yield of 44.18%.

Sources & evidence

ORD record
ord-7040f849d4e74d7f9dce179ed8717aba
Source dataset
uspto-grants-1992_10
Patent number
US05155113

Reaction notes

Loading…