2-Furancarbonyl chloride → HCID 14049651, compound

HRID 466142Notes

Reaction equation

HRID 466142 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6](Cl)=[O:7].[Cl:9][C:10]1[C:11]([OH:17])=[CH:12][C:13](=[O:16])[NH:14][CH:15]=1>N1C=CC=CC=1>[Cl:9][C:10]1[C:11]([O:17][C:6]([C:2]2[O:1][CH:5]=[CH:4][CH:3]=2)=[O:7])=[CH:12][C:13](=[O:16])[NH:14][CH:15]=1

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 54679224Gimeracil

Product 1

HCID 14049651HCID 14049651, compoundYield 34%

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

A 2.15 g quantity of 2-furoyl chloride was added to a suspension of 2.00 g of 5-chloro-4-hydroxy-2-pyridone in 100 ml of pyridine. The same subsequent procedure as in Example 39 was conducted, thereby producing 1.13 g of the title compound in a yield of 34%.

Sources & evidence

ORD record
ord-2569f0681fe24e719118b78b18af0831
Source dataset
uspto-grants-1992_10
Patent number
US05155113

Reaction notes

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