HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyltin trichloride → Dibutyltin dichloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyltin trichloride | HCID 14236 | — |
| Reactant | Butyltricyclohexylstannane | HCID 81516 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | Dibutyltin dichloride | HCID 12688 | — |
| Product | Stannane, chlorotricyclohexyl- | HCID 76539 | — |
Reaction Steps
A solution of equimolar amounts of butyl tricyclohexyltin and butyltin trichloride in commercial xylene was refluxed for 221/2 hours. Analysis of the reaction mixture obtained showed that the reaction had gone to about 89% completion to form predominantly tricyclohexyltin chloride and dibutyltin dichloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04174346 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-c5e415f74b814fec966c82cbe051672a |
| Source note | uspto-grants-1979_11 |