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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 466516Generated: October 30, 2026

Methyl chloroformate → 2,6,7-Trioxabicyclo(2.2.2)octane, 4-(1,1-dimethylethyl)-1-(4-ethynylphenyl)-

https://huagongshe.com/reaction/466516

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl chloroformateHCID 6586—
Reactant1-(4-Ethynylphenyl)-4-propyl-2,6,7-trioxabicyclo(2.2.2)octaneHCID 115223—
ReactantMethyl 3-[4-(4-n-propyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)phenyl]prop-2-ynoateHCID 15021972—
Product2,6,7-Trioxabicyclo(2.2.2)octane, 4-(1,1-dimethylethyl)-1-(4-ethynylphenyl)-HCID 176088—

Reaction Steps

Using the methodology described in (ii) above and starting from (1-(4-ethynylphenyl)-4-n-propyl-2,6,7-trioxabicyclo[2,2,2]octane and methyl chloroformate, methyl 3-[4-(4-n-propyl-2,6,7-trioxabicyclo[2,2,2]oct-1-yl)phenyl]prop-2-ynoate was prepared.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05157029
Source datasetuspto-grants-1992_10
ORD IDord-2e74eb2822b44dfb80a31845967c3178
Source noteuspto-grants-1992_10