HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexanoic Acid → 7-Methyl-2-pentyl-3H-imidazo[4,5-b]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexanoic Acid | HCID 8892 | — |
| Reactant | 4-Methylpyridine-2,3-diamine | HCID 317495 | — |
| Product | 7-Methyl-2-pentyl-3H-imidazo[4,5-b]pyridine | HCID 19814121 | — |
Reaction Steps
The title compound was prepared from 2,3-diamino-4-picoline (0.246 g, 2 mmol) and hexanoic acid (0.25 ml, 2 mmols) according to the procedure described in Step 1 of Example 9. The crude product was purified by flash chromatography on silica-gel using EtOAc-MeOH (9:1) to give the pure product (0.28 g, 69%) as a tan colored solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05157026 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-841ec3cba52e428982d1c07469bac46d |
| Source note | uspto-grants-1992_10 |