HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Hydroxyacetophenone → HCID 178465686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Hydroxyacetophenone | HCID 7469 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | Hydroxylamine dihydrogen phosphate | HCID 167787 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178465686 | HCID 178465686 | 211.8% |
Reaction Steps
A solution was prepared by adding 20.4 g (0.15 mol) of 4-hydroxyacetophenone and 12.9 g (65.6 mmol) of hydroxylamine phosphate to 100 mL of water at 70° C. To the solution was added 16.3 mL of 30% ammonium hydroxide which was then heated at reflux for 0.5 h. White crystals formed upon cooling yielding 21.0 g (92.6%) of 4-hydroxyacetophenone oxime.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05157142 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-c84b1af624f54ac7802438c908485092 |
| Source note | uspto-grants-1992_10 |