2-Ethylhexylamine → HCID 57191275, compound

Participants

Reaction Conditions

Reaction Steps

128.98 Grams (1 mole) of 2-ethyl-1-hexylamine and 500 ml of toluene were charged to a flask equipped with dropping funnel, thermometer, condenser, stirrer, Dean & Stark trap and condenser. The contents of the flask were refluxed for 3 hours to remove water, then cooled to 0° C. 99.6 Grams (1 mole) of butyl isocyanate were charged to the dropping funnel and added during 1 hr. 5 min. to the stirred flask contents. The flask contents remained at 30° C. or less during the addition.

Provenance & Evidence