HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Arecoline → 3-Methoxycarbonyl-1-methyl-4-(3-trifluoromethylphenyl)piperidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Arecoline | HCID 2230 | — |
| Edukt | Benzene, 1-bromo-3-(trifluoromethyl)- | HCID 9817 | — |
| Produkt | 3-Methoxycarbonyl-1-methyl-4-(3-trifluoromethylphenyl)piperidine | HCID 19751261 | — |
Reaktionsschritte
3-methoxycarbonyl-1-methyl-4-(3-trifluoromethylphenyl)piperidine was prepared as the cis/trans mixture from arecoline and 3-bromo-trifluoromethylbenzene as described (J.Org.Chem. 22 (1957) 261). The product was purified by vacuum distillation. B.p. 90°-110° C./0.7 mmHg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05158961 |
| Quelldatensatz | uspto-grants-1992_10 |
| ORD ID | ord-e557129809e44acabf92cdd7ba2da420 |
| Quellennotiz | uspto-grants-1992_10 |