HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopentane → HCID 67638877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopentane | HCID 8057 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 67853206 | HCID 67853206 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67638877 | HCID 67638877 | — |
Reaction Steps
(+-)-trans-3-(3,4-methylenedioxyphenoxymethyl)-1-pentyl-4-(4-pentyloxyphenyl)piperidine hydrochloride was prepared by refluxing 4-(4-hydroxyphenyl)-3-(3,4-methylenedioxyphenoxymethyl)piperidine hydrochloride (0.35 g) with 1-bromopentane (1.8 ml) and K2CO3 (1 g) in abs. ethanol (25 ml) for 2 h. The rinse-up procedure described in example 1 gave the title compound. M.p. 148.2° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05158961 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-84b36cfc92c443c5b39af29ec6bacd45 |
| Source note | uspto-grants-1992_10 |