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HRID467082

反应详情

EQUATION

反应方程式

HRID 467082 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)Cl
HCID31297

Methanesulfonyl chloride

CH3ClO2S

结构：CN(CCc1ccc(N)cc1)Cc1nc2cc(N)ccc2o1
HCID19813431

未命名化合物

PRODUCTS

生成物

1
结构：CN(CCc1ccc(NS(C)(=O)=O)cc1)Cc1nc2cc(NS(C)(=O)=O)ccc2o1
HCID10389165

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

Methanesulphonyl chloride (0.38 g, 3.3 mmole) and N-methyl-N-(5-aminobenzoxazol-2-ylmethyl)-4-aminophenethylamine (see Preparation 1C--0.45 g, 1.5 mmole) in pyridine (20 ml) when reacted together under conditions similar to those of Example 2 gave the title compound, yield from ethanol 0.25 g, m.p. 174°-176°.