HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 14299925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Cerium(III) chloride | HCID 24636 | — |
| Reactant | tert-butyl (2S)-2-formylpyrrolidine-1-carboxylate | HCID 2734674 | — |
| Reactant | Methylorthoformate | HCID 53629101 | — |
| Product | HCID 14299925 | HCID 14299925 | — |
Reaction Steps
tert-Butoxycarbonyl-L-prolinal is acetalized with methyl orthoformate in a 0.4 M solution of cerium chloride in ethanol to give tert-butoxycarbonyl-L-prolinal dimethyl acetal as a colorless syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05158970 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-6729746f35f945bda33a2b3bf82c39e2 |
| Source note | uspto-grants-1992_10 |