HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 19813529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 14839562 | HCID 14839562 | — |
| Catalyst | Silver(II) oxide | HCID 92152 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 19813529 | HCID 19813529 | — |
Reaction Steps
To a solution of 17.42 g (0.07 mole) of 1,4-dimethoxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro naphthalene, obtained in Example VIa, in 340 cm3 of dioxane, cooled to +5° C., there are added, with stirring, 34.7 g (0.28 mole) of silver oxide, AgO(II), then rapidly drop-by-drop, 70 cm3 (0.42 mole) of 6N HNO3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05158977 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-66e063224ed14bcab917ffa7344b7f93 |
| Source note | uspto-grants-1992_10 |