Sodium Hydroxide → HCID 86744014, compound

HRID 467171Notes

Reaction equation

[C:1]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])(=[O:7])/[CH:2]=[CH:3]\[C:4]([O-:6])=[O:5].[OH-].[Na+].O.O.C([O-])(=O)C.[Zn+2:29].C([O-])(=O)C>CC(C)=O>[C:1]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])(=[O:7])/[CH:2]=[CH:3]\[C:4]([O-:6])=[O:5].[Zn+2:29].[CH2:9]([O:8][C:1](=[O:7])/[CH:2]=[CH:3]\[C:4]([O-:6])=[O:5])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

Conditions

Temperature: 50 °C

Procedure

To a 12 percent weight by volume (w/v) acetone suspension of the monododecyl maleate heated to 50° C. is added 1.0 molar equivalent sodium hydroxide as a 10 percent w/v aqueous solution. After the stirred suspension clears, 0.5 molar equivalent zinc acetate dihydrate as a saturated aqueous solution is added with stirring. The supernatant liquid is separated from the precipitated zinc dodecyl maleate.

Workup

customThe supernatant liquid is separated from the precipitated zinc dodecyl maleate

Sources & evidence

ORD record: ord-aebd4649a634440c8f04d4c2d42c45d3
Source dataset: uspto-grants-1992_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05159035

Reaction notes

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