Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylbenzene | HCID 7500 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | HCID 131716422 | HCID 131716422 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 131716420 | HCID 131716420 | — |
Reaction Steps
To a 10 percent w/v ethylbenzene solution of 135 g of 1-(2-hydroxyethyl)-2-isostearyl-3-benzylimidazolinium chloride at 20° C. is added 1.1 molar equivalents (24.5 g) of pyridine followed by dropwise addition of 1.3 molar equivalents (38.3 g) of methacryloyl chloride. The solution is stirred for 4 hours at 20° C. followed by separation of the supernatant liquid and the ethylbenzene removed to give an oil of 1-(2-methacryloxyethyl)-2-isostearyl-3-benzylimidazolinium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05159035 |
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| Source dataset | uspto-grants-1992_10 |
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| ORD ID | ord-9fd6c6931fe041879122fd7408172c70 |
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| Source note | uspto-grants-1992_10 |
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