Sodium Hydroxide → HCID 86744017, compound

HRID 467175Notes

Reaction equation

HRID 467175 reaction equation
[C:1]([O:9][CH2:10][CH:11]([CH2:16][CH3:17])[CH2:12][CH2:13][CH2:14][CH3:15])(=[O:8])[C:2]([CH2:4][C:5]([O-:7])=[O:6])=[CH2:3].[OH-].[Na+].O.O.C([O-])(=O)C.[Zn+2:26].C([O-])(=O)C>>[C:1]([O:9][CH2:10][CH:11]([CH2:16][CH3:17])[CH2:12][CH2:13][CH2:14][CH3:15])(=[O:8])[C:2]([CH2:4][C:5]([O-:7])=[O:6])=[CH2:3].[Zn+2:26].[CH2:16]([CH:11]([CH2:12][CH2:13][CH2:14][CH3:15])[CH2:10][O:9][C:1](=[O:8])[C:2]([CH2:4][C:5]([O-:7])=[O:6])=[CH2:3])[CH3:17]

Participants

4

Reactant 3

HCID 14798Sodium HydroxideHCID 2724192Zinc acetate (USP)HCID 20077216HCID 20077216, compound

Product 1

HCID 86744017HCID 86744017, compound

Procedure

To a 30 percent w/v aqueous dispersion of the mono-2-ethylhexyl itaconate is added 1 molar equivalent of sodium hydroxide as a 10 percent w/v aqueous solution (800 ml). After the stirred suspension clears, 0.5 molar equivalent (219 g) of zinc acetate dihydrate as a saturated aqueous solution is added with stirring. The supernatant liquid is separated from the precipitated zinc 2-ethylhexyl itaconate (6A).

Workup

  1. customThe supernatant liquid is separated from the precipitated zinc 2-ethylhexyl itaconate (6A)

Sources & evidence

ORD record
ord-3aad49b6c80a4de982b5b928d383d04c
Source dataset
uspto-grants-1992_10
Patent number
US05159035

Reaction notes

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