HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 75153364, compound → HCID 46221559, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 75153364 | HCID 75153364 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | HCID 46221559 | HCID 46221559 | 96% |
Reaction Steps
395 g of 5-Phenyl-2-n-propyl-penta-2,4-dienal from Synthesis Example 1.1 were combined with 14 g of Raney-Ni and hydrogenated at a hydrogen pressure of 20 bar and at a temperature of 120° C. After 20 hours the reaction was finished. The catalyst was removed and the product distilled. 365 g (content 96%) of 5-phenyl-2-n-propyl-pentanol are obtained. Yield: 93.6% of theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623340B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-53ed7b752b594c35969348ab4c78c29f |
| Source note | uspto-grants-2014_01 |