HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15830832, compound → HCID 15174002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15830832 | HCID 15830832 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | HCID 15174002 | HCID 15174002 | 99.5% |
Reaction Steps
100 g of 2,4-Dimethyl-5-phenyl-pentanol (obtained as described in EP 0 908 439) combined with 2 g Ru on aluminium oxide (Ru content: 5 wt. %) were hydrogenated in 80 ml cyclohexane at a hydrogen pressure of 22 bar and at a temperature of 105° C. After 18 hours the reaction was finished. The catalyst was removed and the product distilled. 100 g (content: 99.5%) of 5-cyclohexyl-2,4-dimethyl-pentanol were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623340B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-71ca6a222bd84cf5a42d8258f9f44f25 |
| Source note | uspto-grants-2014_01 |