HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-5-phenylpentanol → Cyclohexanepentanol, .beta.-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-5-phenylpentanol | HCID 5463791 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Cyclohexanepentanol, .beta.-methyl- | HCID 44192644 | 99.6% |
Reaction Steps
1200 g of 2-Methyl-5-phenyl-pentanol (Rosaphen™, supplier: Symrise) combined with 22 g Pd on activated carbon (Pd content: 5 wt. %) were hydrogenated at a hydrogen pressure of 50 bar and at a temperature of 120° C. After 30 hours the reaction was finished. The catalyst was removed and the product distilled. 1170 g (content: 99.6%) of 5-cyclohexyl-2-methyl-pentanol were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623340B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-54cd8deb2c9442da8c688710a38a0786 |
| Source note | uspto-grants-2014_01 |