HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium iodide → HCID 70099812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium iodide | HCID 66321 | — |
| Reactant | HCID 70097488 | HCID 70097488 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 70099812 | HCID 70099812 | — |
Reaction Steps
To a solution of methyl 6-(6-cyclopropyl-3-(pyrimidin-5-ylamino)pyrazine-2-carboxamido)-2,3-dimethylbenzoate (0.05 g, 119 μmol) in pyridine (1 ml) at r.t under an argon atmosphere was added lithium iodide (125 mg, 932 μmol). The mixture was heated at 100° for 16 hr. The solvent was evaporated. The crude product was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623866B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-2d1ba1f522a14e97b97d470472926226 |
| Source note | uspto-grants-2014_01 |