HuagongsheHuagongshe Chemistry Print Report · For research reference only
NoName_4581 → HCID 54760761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | NoName_4581 | HCID 143443 | — |
| Reactant | 4-{[6-Cyclopropyl-3-(pyrimidin-5-ylamino)-pyrazine-2-carbonyl]-amino}-2-methyl-2H-pyrazole-3-carboxylic acid | HCID 70098073 | — |
| Product | HCID 54760761 | HCID 54760761 | — |
Reaction Steps
The product was obtained starting from 4-{[6-cyclopropyl-3-(pyrimidin-5-ylamino)-pyrazine-2-carbonyl]-amino}-2-methyl-2H-pyrazole-3-carboxylic acid (50 mg, 131 μmol; example 236, step 3) and 2-aminocyclopentanol (15 mg, 140 μmol) according to the method described in example 64, step 6 after purification by preparative HPLC using an acetonitrile/water gradient as yellow solid (24 mg, 40%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08623866B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-6a26e622870c450fbf8ee79e9d5bb026 |
| Source note | uspto-grants-2014_01 |