Ethanol hydrochloride → HCID 178472547, compound

HRID 467950Notes

Reaction equation

HRID 467950 reaction equation
[CH2:1]([O:8][C:9]([NH:11][CH2:12][CH2:13][C:14]([NH:16][C@H:17]([C:24]([OH:26])=[O:25])[CH2:18][C:19]1[N:23]=[CH:22][NH:21][CH:20]=1)=[O:15])=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:27](O)[CH3:28].Cl>C(O)C>[CH2:27]([O:25][C:24](=[O:26])[C@H:17]([CH2:18][C:19]1[N:23]=[CH:22][NH:21][CH:20]=1)[NH:16][C:14](=[O:15])[CH2:13][CH2:12][NH:11][C:9]([O:8][CH2:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)=[O:10])[CH3:28]

Participants

4

Reactant 2

HCID 21887872Ethanol hydrochlorideHCID 1785208513-(Benzyloxycarbonylamino) propionyl-L-histidine

Product 1

HCID 178472547HCID 178472547, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A 1 L round-bottom flask, under nitrogen atmosphere, is loaded with 40 g of 3-(benzyloxycarbonylamino) propionyl-L-histidine, 200 g of absolute ethanol and 80 g of an 8M HCl ethanol solution.

Sources & evidence

ORD record
ord-48b6915fe4514c7cb20975e969c22d5f
Source dataset
uspto-grants-2014_01
Patent number
US08623900B2

Reaction notes

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