HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178421680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Thiocarbohydrazide | HCID 2724189 | — |
| Reactant | (1-Methylcyclopropyl)-glyoxylic acid tert-butylamide | HCID 20385839 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178421680 | HCID 178421680 | — |
Reaction Steps
183 grams of (1-methyl-cyclopropyl)-glyoxalic acid-tert.-butylamide and 112 grams of thiocarbohydrazide were added to a mixture of 1 liter of 1 normal HCl and 1 liter of ethanol. The mixture was boiled under reflux for 8 hours, cooled, diluted with 2 liters of water and the crystals filtered off with suction. There were obtained white crystals with a yellow luster which were dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04175188 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-e471648b4ae44be4b25f0eae45b4618f |
| Source note | uspto-grants-1979_11 |