HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 468407Generated: October 30, 2026
Dimethylacetamide → HCID 57470203, compound
https://huagongshe.com/reaction/468407
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Reactant | Ethyl 2-methyl-3,5-dinitrobenzoate | HCID 43386560 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 57470203 | HCID 57470203 | 48% |
Reaction Steps
A mixture of ethyl 2-methyl-3,5-dinitrobenzoate (35 g, 0.14 mol) and DMA (32 g, 0.27 mol) in DMF (200 mL) was heated at 100° C. for 5 h. The mixture was poured into ice-water and the precipitated solid was filtered and washed with water to give (E)-ethyl 2-(2-(dimethylamino)vinyl)-3,5-dinitrobenzoate (11 g, 48%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08623905B2 |
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| Source dataset | uspto-grants-2014_01 |
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| ORD ID | ord-b55aa5946bcc4f87994794deee99f608 |
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| Source note | uspto-grants-2014_01 |
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