HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 468409Generated: October 26, 2026
Dimethylformamide → (E)-2-(5-fluoro-2,4-dinitrophenyl)-N,N-dimethylethenamine
https://huagongshe.com/reaction/468409
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Reactant | 1-Fluoro-5-methyl-2,4-dinitrobenzene | HCID 520705 | — |
| Solvent | Water | HCID 962 | — |
| Product | (E)-2-(5-fluoro-2,4-dinitrophenyl)-N,N-dimethylethenamine | HCID 15022335 | 63% |
Reaction Steps
A mixture of 1-fluoro-5-methyl-2,4-dinitro-benzene (10 g, 50 mmol), DMA (12 g, 100 mmol) and DMF (50 nit) was heated at 100° C. for 4 h. The solution was cooled and poured into water. The precipitated red solid was collected, washed with water, and dried to give (E)-2-(5-fluoro-2,4-dinitrophenyl)-N,N-dimethylethenamine (8.0 g, 63%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08623905B2 |
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| Source dataset | uspto-grants-2014_01 |
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| ORD ID | ord-b8df435da39b42fd8e4410c5ca578235 |
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| Source note | uspto-grants-2014_01 |
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