Diisopropylcarbodiimide → HCID 67226568, compound

Participants

Reaction Steps

A solution of the alcohol 4 (685 mg, 3.26 mmol), the acid 2 (932 mg, 4.57 mmol), DIC (680 μl, 4.57 mmol) and DMAP (39 mg, 0.32 mmol) was stirred overnight at room temperature. The mixture was then filtered and concentrated. Flash chromatography on silica gel (EtOAc/pentane 1/1) afforded compound 5 as an oil (1.06 g, 82%).

Provenance & Evidence