HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-Iodophenoxy)-1,3-thiazole → 2-[3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]-1,3-thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-Iodophenoxy)-1,3-thiazole | HCID 60753841 | — |
| Reactant | 2-[4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-2H-tetrazole | HCID 70664586 | — |
| Product | 2-[3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]-1,3-thiazole | HCID 70664594 | — |
Reaction Steps
The title compound (1.33 g) was prepared as a crude brown solid from 2-(3-iodophenoxy)-1,3-thiazole (500 mg, 1.65 mmol) using a procedure analogous to that described for 2-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-2H-tetrazole, Example 1, Step A. MS (LCMS) m/z 304.0 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08624034B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-28f4ec0918684317b453ee5305a36077 |
| Source note | uspto-grants-2014_01 |