HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 4-Hydroxyphenylglycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Ammonium formate | HCID 2723923 | — |
| Reactant | Sodium glyoxylate | HCID 23662273 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-Hydroxyphenylglycine | HCID 92143 | 34.2% |
Reaction Steps
36.9 g of sodium glyoxylate, 61.3 g of ammonium formate, 60 g of phenol and 130 g of water are treated in the same manner as described in Example 1. 18.5 g of DL-p-hydroxyphenylglycine are thereby obtained as crystals. Yield: 34.2% M.p. 225°-228° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04175206 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-6568d7eac24a4c50a34ceef5bb51d78a |
| Source note | uspto-grants-1979_11 |