HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo(B)Thiophene-2-Boronic Acid → HCID 58557010, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo(B)Thiophene-2-Boronic Acid | HCID 2359 | — |
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Glyoxylic acid, monohydrate | HCID 15620607 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 58557010 | HCID 58557010 | — |
Reaction Steps
A mixture of benzo[b]thiophen-2-ylboronic acid (500 mg, 2.81 mmol), aniline (240 μl, 2.81 mmol), and 2-oxoacetic acid hydrate (259 mg, 2.81 mmol) in acetonitrile (20 ml) was stirred at room temperature for three days. The solvent was evaporated to dryness and the crude was used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629160B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-10b4546754704034a4bb25b37a2f45bf |
| Source note | uspto-grants-2014_01 |