HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyaniline → HCID 58556984, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Reactant | (1-Benzothiophen-3-yl)boronic acid | HCID 2776344 | — |
| Reactant | Glyoxylic acid, monohydrate | HCID 15620607 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 58556984 | HCID 58556984 | — |
Reaction Steps
A mixture of 3-methoxyaniline (400 mg, 3.25 mmol), benzo[b]thiophen-3-ylboronic acid (578 mg, 3.25 mmol), and 2-oxoacetic acid hydrate (299 mg, 3.25 mmol) in acetonitrile (30 ml) was stirred at room temperature overnight. The solvent was removed under vacuum and the crude was used us such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629160B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-68eacc4c61b74a78b44abaa6024ca954 |
| Source note | uspto-grants-2014_01 |