反应详情

The product of Example 11B (50.6 mg) and (adamantan-1-yl)acetyl chloride (54 mg, 0.25 mmol) were treated as in Example 6 to give the title compound (69 mg, 0.17 mmol) as a white solid. 1H NMR (300 MHz, DMSO-d6) δ 11.47 (s, 1H), 8.44 (dd, 1H), 8.18-7.98 (m, 3H), 2.08 (s, 2H), 1.99-1.92 (m, 3H), 1.75-1.55 (m, 12H); MS (DCI) M/Z 423.3 (M+NH4)+.