1-Adamantaneacetic acid → HCID 53237968, compound

Participants

Reaction Steps

The product from Example 35E and 2-(adamant-1-yl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (500 MHz, DMSO-d6) δ ppm 1.49-1.76 (m, 12H) 1.86-1.99 (m, 3H) 2.06 (s, 2H) 7.39 (dd, J=9.46, 2.44 Hz, 1H) 7.52-7.67 (m, 5H) 7.71-7.94 (m, 1H) 8.49 (dd, J=8.85, 5.49 Hz, 1H) 11.29 (s, 1H); MS (ESI) m/z 432 (M+H)+.

Provenance & Evidence