HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-N,N-dimethylaminophenylacetic acid → HCID 53238207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-N,N-dimethylaminophenylacetic acid | HCID 152203 | — |
| Reactant | 2-amino-4-(trifluoromethyl)phthalazin-1(2H)-one | HCID 67161111 | — |
| Product | HCID 53238207 | HCID 53238207 | — |
Reaction Steps
The product from Example 11B and 2-[4-(dimethylamino)phenyl]acetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.43 (dd, J=7.9, 1.3 Hz, 1H), 8.13-8.17 (m, 1H), 8.04-8.08 (m, 2H), 7.38-7.40 (m, 2H), 7.19-7.21 (m, 2H), 3.70 (s, 2H), 3.05 (s, 6H); MS (ESI−) M/Z 389 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-bf6575eea2f04435ad67a4c8f41d1368 |
| Source note | uspto-grants-2014_01 |