beta-Phenylisovaleric acid → HCID 53238431, compound

Participants

Reaction Steps

The product of Example 11B and 3-methyl-3-phenylbutanoic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.58-11.60 (bs, 1H), 8.43 (dd, J=7.9, 1.3 Hz, 1H), 8.11-8.15 (m, 1H), 7.97-8.07 (m, 2H), 7.43-7.46 (m, 2H), 7.28-7.36 (m, 2H), 7.16-7.21 (m, 1H), 2.66 (s, 2H), 1.46 (s, 6H); MS (ESI) m/z 390 (M+H)+.

Provenance & Evidence