(4-Chlorophenyl)acetic acid → HCID 67160587, compound

Participants

Reaction Steps

The product of Example 74A and 2-(4-chlorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.55 (s, 1H), 8.32 (dd, J=7.9, 1.4 Hz, 1H), 8.12 (d, J=8.1 Hz, 1H), 7.97-8.02 (m, 1H), 7.87-7.92 (m, 1H), 7.37-7.47 (m, 4H), 3.68 (s, 2H), 3.22-3.29 (bs, 1H), 1.87-1.92 (m, 2H), 1.78-1.82 (m, 2H), 1.70-1.76 (m, 1H), 1.41-1.54 (m, 4H), 1.18-1.29 (m, 1H); MS (ESI) m/z 396 (M+H)+.

Provenance & Evidence