HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → Ethyl 4-(3-bromopropyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 4-(3-bromopropyl)benzoic acid | HCID 237785 | — |
| Solvent | Water | HCID 962 | — |
| Product | Ethyl 4-(3-bromopropyl)benzoate | HCID 12748306 | — |
Reaction Steps
A mixture of p-(3-bromopropyl)benzoic acid (100.8 g.; 0.41 mole), benzene (290 ml.), ethanol (60 ml.) and concentrated sulfuric acid (1.4 ml.) is heated under reflux under a Dean and Stark constant water separator until the evolution of water ceases. The time required is 23 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04175203 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-6ac9d5067d6f418298385d3664eb84ef |
| Source note | uspto-grants-1979_11 |