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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 469605Generated: October 31, 2026

4-Methoxyphenylacetic Acid → HCID 53238892, compound

https://huagongshe.com/reaction/469605

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Methoxyphenylacetic AcidHCID 7690—
Reactant2-amino-4-(4-chlorophenyl)phthalazin-1(2H)-oneHCID 67161367—
ProductHCID 53238892HCID 53238892—

Reaction Steps

The product of Example 86A and 2-(4-methoxyphenyl)acetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.40-8.42 (m, 1H), 7.88-8.03 (m, 2H), 7.71-7.74 (m, 1H), 7.58-7.68 (m, 4H), 7.29-7.31 (m, 2H), 6.90-6.93 (m, 2H), 3.74 (s, 3H), 3.62 (s, 2H); MS (APCI+) M/Z 420 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629143B2
Source datasetuspto-grants-2014_01
ORD IDord-079008e2cae546859ece98aa0e3c2dcf
Source noteuspto-grants-2014_01