HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyphenylacetic acid → HCID 53238890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyphenylacetic acid | HCID 127 | — |
| Reactant | 2-amino-4-(4-chlorophenyl)phthalazin-1(2H)-one | HCID 67161367 | — |
| Product | HCID 53238890 | HCID 53238890 | — |
Reaction Steps
The product of Example 86A and 2-(4-hydroxyphenyl)acetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.38-8.42 (m, 1H), 7.95-8.02 (m, 2H), 7.72-7.75 (m, 1H), 7.60-7.67 (m, 4H), 7.17-7.19 (m, 2H), 6.73-6.75 (m, 2H), 3.57 (s, 2H); MS (ESI−) M/Z 404 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-ab9fcfcba5234e18a32a736f49e5402c |
| Source note | uspto-grants-2014_01 |