m-Tolylacetic acid → HCID 53238661, compound

Participants

Reaction Steps

The product of Example 86A and 2-(3-methylphenyl)acetic acid were treated using a method similar to that described in Example 57 to give the title compound. 1H NMR (500 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.41-8.43 (m, 1H), 7.93-8.04 (m, 2H), 7.72-7.74 (m, 1H), 7.60-7.66 (m, 4H), 7.24 (t, J=7.5 Hz, 1H), 7.19-7.21 (m, 1H), 7.16-7.19 (m, 1H), 7.08-7.12 (m, 1H), 3.65 (s, 2H), 2.31 (s, 3H); MS (ESI−) M/Z 402 (M−H)−.

Provenance & Evidence