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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 469617Generated: October 30, 2026

(4-Chlorophenyl)acetic acid → HCID 53238658, compound

https://huagongshe.com/reaction/469617

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(4-Chlorophenyl)acetic acidHCID 15880—
Reactant2-amino-4-(4-chlorophenyl)phthalazin-1(2H)-oneHCID 67161367—
ProductHCID 53238658HCID 53238658—

Reaction Steps

The product of Example 86A and 2-(4-chlorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.63-11.81 (bs, 1H), 8.39-8.42 (m, 1H), 7.90-8.03 (m, 2H), 7.69-7.76 (m, 1H), 7.60-7.66 (m, 4H), 7.34-7.46 (m, 4H), 3.71 (s, 2H); MS (ESI+) m/z 424 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629143B2
Source datasetuspto-grants-2014_01
ORD IDord-2cf89dfbbf4144cd948ab041580c4fa5
Source noteuspto-grants-2014_01