trans-2-Phenyl-1-cyclopropanecarbonyl chloride → HCID 67161048, compound

Participants

Reaction Steps

The product from Example 86A and trans-2-phenyl-1-cyclopropanecarbonyl chloride were treated using a method similar to that described in Example 53 to give the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 11.69 (s, 1H), 8.39-8.43 (m, 1H), 7.88-8.06 (m, 2H), 7.68-7.82 (m, 1H), 7.64 (s, 4H), 7.28-7.36 (m, 2H), 7.18-7.25 (m, 3H), 2.36-2.45 (m, 1H), 2.05-2.14 (m, 1H), 1.37-1.56 (m, 2H); MS (ESI+) M/Z 416 (M+H)+.

Provenance & Evidence