HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorophenylacetic acid → HCID 67160788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorophenylacetic acid | HCID 145424 | — |
| Reactant | HCID 67160366 | HCID 67160366 | — |
| Product | HCID 67160788 | HCID 67160788 | — |
Reaction Steps
The product of Example 125A and 2-(3,5-difluorophenyl)acetic acid were processed using a method similar to that described in Example 17C to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.79 (s, 1H), 8.40-8.43 (m, 1H), 7.91-8.05 (m, 2H), 7.71-7.75 (m, 1H), 7.63-7.68 (m, 2H), 7.56-7.63 (m, 2H), 7.07-7.22 (m, 3H), 3.78 (s, 2H); MS (ESI+) m/z 426 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08629143B2 |
| Source dataset | uspto-grants-2014_01 |
| ORD ID | ord-32dc9bdcf7bf457cbf7d0758957e336b |
| Source note | uspto-grants-2014_01 |