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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 469628Generated: October 30, 2026

3,5-Difluorophenylacetic acid → HCID 67160072, compound

https://huagongshe.com/reaction/469628

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3,5-Difluorophenylacetic acidHCID 145424—
ReactantHCID 67160399HCID 67160399—
ProductHCID 67160072HCID 67160072—

Reaction Steps

The product of Example 129A and 2-(3,5-difluorophenyl)acetic acid were treated using a method similar to that described in Example 17C to give the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.77-11.79 (bs, 1H), 8.40-8.43 (m, 1H), 7.90-8.03 (m, 2H), 7.69-7.74 (m, 1H), 7.63-7.69 (m, 2H), 7.38-7.43 (m, 2H), 7.06-7.21 (m, 3H), 3.77-3.78 (bs, 2H); MS (APCI+) M/Z 410 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08629143B2
Source datasetuspto-grants-2014_01
ORD IDord-476b3c89d1704e4f93a916329c5225d2
Source noteuspto-grants-2014_01