1-Adamantaneacetyl chloride → HCID 67160730, compound

Participants

Reaction Steps

The product of Example 147A and 2-(adamantan-1-yl)acetyl chloride were treated using a method similar to that described in Example 1C to give the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.31 (s, 1H), 8.42-8.45 (m, 1H), 7.96-8.01 (m, 2H), 7.93-7.97 (m, 2H), 7.83-7.86 (m, 2H), 7.72-7.76 (m, 1H), 2.06 (s, 2H), 1.93-1.96 (m, 3H), 1.58-1.73 (m, 12H); MS (APCI+) M/Z 482 (M+H)+.

Provenance & Evidence