1-Adamantaneacetyl chloride → HCID 53236156, compound

Participants

Reaction Steps

The product from Example 151A and (adamantan-1-yl)acetyl chloride were treated using a method similar to that described in Example 1C to give the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 11.23 (s, 1H), 8.39-8.42 (m, 1H), 7.88-8.02 (m, 2H), 7.75-7.78 (m, 1H), 7.52-7.55 (m, 2H), 7.11-7.14 (m, 2H), 3.85 (s, 3H), 2.05 (s, 2H), 1.94-1.97 (m, 3H), 1.59-1.70 (m, 12H); MS (ESI+) M/Z 444 (M+H)+.

Provenance & Evidence