HCID 10467993, compound → HCID 67160201, compound

HRID 469655Notes

Reaction equation

HRID 469655 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[C:13](=[O:20])[NH:12][N:11]=2)=[CH:6][CH:5]=1)([CH3:3])[CH3:2].C1(P(O[NH2:36])(C2C=CC=CC=2)=O)C=CC=CC=1>>[NH2:36][N:12]1[N:11]=[C:10]([C:7]2[CH:6]=[CH:5][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:9][CH:8]=2)[C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[C:13]1=[O:20]

Participants

3

Reactant 2

HCID 10467993HCID 10467993, compoundHCID 10955453O-(Diphenylphosphinyl)hydroxylamine

Product 1

HCID 67160201HCID 67160201, compound

Procedure

4-(4-Isopropylphenyl)phthalazin-1(2H)-one was treated with O-(diphenylphosphoryl)hydroxylamine using a method similar to that described in Example 1B to give the title compound. MS (APCI+) M/Z 279 (M+H)+.

Sources & evidence

ORD record
ord-2c22bcd268714a8f9041f00f233eb3c1
Source dataset
uspto-grants-2014_01
Patent number
US08629143B2

Reaction notes

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